GSECARS Xray Microprobe for Earth and Environmental Sciencegsecars X射线微探针对地球和的环境科学.pptVIP

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GSECARS Xray Microprobe for Earth and Environmental Sciencegsecars X射线微探针对地球和的环境科学.ppt

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GSECARS Xray Microprobe for Earth and Environmental Sciencegsecars X射线微探针对地球和的环境科学

21-Jan-2004 GSECARS X-ray Microprobe for Earth and Environmental Science GSECARS XRF/XAFS Microprobe Station X-ray Fluorescence Detectors Arsenic/Iron in cattail roots: XRF tomography X-ray Fluorescence Tomography: Overview Fluorescence Tomography: Experimental Setup Fluorescence Tomography: Sinograms Fluorescence Tomogram Slices of Cattail Roots As oxidation tomograms for Cattail Roots Future Directions and Microprobe Improvements Matthew Newville, Peter Eng, Steve Sutton, Mark Rivers Consortium for Advanced Radiation Sources (CARS) University of Chicago, Chicago, IL X-ray Absorption (XANES / EXAFS) Objective for Earth and Environmental Sciences: X-ray Microprobe techniques: oxidation state of selected element near-neighbor distances and coordination numbers abundance and spatial correlations of heavy elements X-ray Fluorescence (XRF), Fluorescence Mapping Determine chemical associations, speciation, and structure of heavy elements on heterogeneous samples: soils, sediments, aggregates, plant material, isolated inclusions, or contaminants. Focusing: Kirkpatrick-Baez mirrors: Rh-coated Si, typically using 3x3mm spot sizes, at 50mm from end of mirrors. Incident Beam: LN2 cooled Si (111) Sample Stage: x-y-z stage, 1mm resolution Samples in air or He, typically Fluorescence detector: 16-element Ge detector / DXP electronics, Lytle Detector, or Wavelength Dispersive Spectrometer Data Collection: custom software for XRF, mapping and XAFS, based on EPICS. Optical Microscope: 5x to 50x objective to external video system. Slits: typically 200 to 300 mm, accepting ~20% of undulator beam at 50m from source. The table-top Kirkpatrick-Baez mirrors use four-point benders and flat, trapezoidal mirrors to dynamically form an ellipsis. They can focus a 300x300mm beam to 1x1mm. With a typical working distance of 100mm, and a focal distance and spot-size independent of energy, they are ideal for micro-XRF and micro-EXAFS. We use Rh-coated silicon for horizontal and