钛铬氧化物纳米结构的水热合成及性能分析-hydrothermal synthesis and properties analysis of titanium-chromium oxide nanostructures.docx

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钛铬氧化物纳米结构的水热合成及性能分析-hydrothermal synthesis and properties analysis of titanium-chromium oxide nanostructures.docx

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钛铬氧化物纳米结构的水热合成及性能分析-hydrothermal synthesis and properties analysis of titanium-chromium oxide nanostructures

西南科技大学硕士研究生学位论文第II页AbstractMetaloxidenanomaterialshavebeenwidelyusedascatalysis,gassensitivematerial,biomedicalmaterialandlithiumionbatteryduetotheiruniquephysicalandchemicalproperties.Thestructureandmorphologyofmetaloxidenanomaterialshaveveryimportantinfluenceonperformance.Therefore,adoptingthefeasiblesynthesismethodandexploringtheirgrowthmechanismshouldbeakeyprerequisitetounderstandtherelationbetweenstructureandperformanceofnanomaterialsandindustrialapplications.Inthispaper,aseriesofnewsynthesismethodsofnanosizedTiO2,BaTiO3,Cr2O3andCr2O3/graphenecompositehavebeendeveloped.Theirreactionmechanismshavebeenexplored.Lithiumionbatteryperformancesofselectedsampleshavebeentested.Alotofresearchandexperimenthavemadesomemeaningfulresults.Byahydrothermalmethod,TiO2hollownanosphereshavebeensuccessfullysynthesizedunderDMFandTFAassistance.ThesampleswerecharacterizedbyX-Raydiffraction,fieldemissionscanningelectronmicroscopyandenergydispersiveX-rayspectrom.TiO2hollownanospherevariousnanostructuresmorphologieshavebeeninvestigatedbychangingthehydrothermaltime,andCrdopedTiO2core-shellstructurematerialshavebeensuccessfullysynthesizedbyusingCr(NO3)3?9H2O.Finally,Lithiumionbatteryperformancesofas-preparedsampleshavebeentested.Inthehydrothermalsystem,BaTiO3nanocrystallinehavebeencontinuouslysynthesizedunderthemineralizerassistance.TheproductswerecharacterizedbyX-Raydiffraction,fieldemissionscanningelectronmicroscopyandhighresolutiontransmissionelectronmicroscopy.Titaniumsource,mineralizer,hydrothermaltimeandrecycletimeshavebeeninvestigatedinpresentexperiment.Atlast,weproposedafeasibleroutetosynthesizeBaTiO3nanocrystallineforindustrialapplications.Byasolvothermalmethod,Cr2O3hollownanosphereshavebeensuccessfullysynthesizedunderoxalicacidandPEG-400assistance.Inthesystem,webelievethatthePEG-400mayplayacertainguidingroleforthegrowthofthecrystal.ThesampleswerecharacterizedbyXRD,FE-SEM,EDX,TGAandRaman,andweproposedapossibleformationmechanismaccordingtotheresults.Graphiteoxidewassynthesizedfromn

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钛铬氧化物纳米结构的水热合成及性能分析-hydrothermal synthesis and properties analysis of titanium-chromium oxide nanostructures.docx