稀土掺质yagysgg纳米材料的制备及性能的研究-preparation and properties of rare earth doped yagysgg nano - material.docx

山东大学硕士学位论文溶胶的制备········································……通凝胶的干燥和热处理·······························……遵……互微结构与性能表征········……”……·····························图谱分析·············································热分析·····················································……碑红外吸收光谱分析········································……碑表征·················································……碑，夸一纳米材料的制备与表征···························……石，互纳米材料的制备和热处理·················……石，溶胶的制备·······························……石十，护凝胶的干燥和热处理·····················……石互微结构与性能的表征·········································……石一粉末衍射············································……石红外光谱分析············································……石表征···················································……石荧光光谱分析……················……‘······················第五章透明陶瓷的烧结··················································…………互一引言·········，························································……互一实验··································································圣一性能表征·····························································……石夸表征······································……”········芍观察…………······················，································第六章结论·································································……石夸一主要结论············································……石夸一主要创新点···········································……石夸一有待进一步研究的内容·····························……石参考文献·················································……石致谢……···········、··················……石发表学位论文·····························……众，口目县山东大学硕士学位论文摘要、、、晶体是当前广泛应用的最重要的激光基质材料目前这类石。，，、，。榴石稀土掺质的晶体多是用提拉法生长出来的这种方法成本高昂工艺复杂，，。速度慢生长周期长掺杂浓度低且难于制备掺杂均匀的大尺寸单晶由于受，到尺寸的限制激光输出功率也难以提高其更广阔的应用受到一定限制，，年日本电通迅大学激光科学研究所等人首次报道了利用高质量的，透明陶瓷材料研制的阵列式激光器其斜率效率高达光一光转换效，。，、率为可与晶体激光器的效率相比拟，。，制备性能优良的透明陶瓷材料首要条件是具有高质量的粉料即粒度均匀、。化学纯度高分散性好的纳米粉料为此高质量的纳米粉料的制备就成为制备，透明陶瓷的关键同时高质量的纳米粉也是高质量单晶生长的最好原料，本文对相关的纳米材料及制备技术进行了大量的调研和分析在，此基础上采用溶胶一凝胶法一制备了和石榴石结构的，纳米多晶粉体材料以及稀土离子掺杂的和纳米多晶粉体材料的研制通，过不同的表征手段研究了热处理温度与微结构及性能的关系得到了一些创新性。成果本论文的主要研究内容和结论如下、·。一以飞珑。场比。和柠