水热法制备高折射率氧化铁薄膜的研究--毕业论文设计.docVIP

PAGE 水热法制备高折射率氧化铁薄膜的研究 摘要:本文以FeCl3·6H2O为原料，采用水热法在玻璃基质上制备高折射率的氧化铁纳米薄膜。研究了反应温度温度、反应时间、pH、填充度，这些因素对所制备纳米氧化铁薄膜折射率的影响。采用自动椭圆偏振仪测试手段对氧化铁纳米膜进行了折射率和膜厚的表征分析。结果表明，水热法制备的薄膜最佳的水热工艺条件是在pH=11、填充度为70 %、水热温度160 ℃ 关键字：水热法，纳米氧化铁薄膜，高折射率 Preparation of Ferric Oxide Films with High Refractive by Hydrothermal Synthesis Lv xiao-xia College of Abstract: Nanometer ferric oxide films were prepared from six hydrated ferric chloride by hydrothermal method. The effects of hydrothermal temperature, reaction time, compactedness and pH on Three iron oxide films were researched, and the ellipsometer was used to characterize the thickness of nanometer Three iron oxide films and high refractive index. The results show that the optimum hydrothermal technological condition is temperature of 160 ℃, hydrothermal time of 4 h, pH of 11 and compactedness of 70 %. Under the optimum condition, the thickness of the films with well-developed crystalline is 130 nm, the refractive index can up to 2.490, the surface of films is quite flat and well-distribute Key words: Hydrothermal method, Nanometer Three iron oxide film, High refractive index 目 录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc326048366 一、引言 PAGEREF _Toc326048366 \h 1 HYPERLINK \l _Toc326048367 （一）光化学的应用 PAGEREF _Toc326048367 \h 1 HYPERLINK \l _Toc326048368 1．国际上光化学的研究 PAGEREF _Toc326048368 \h 1 HYPERLINK \l _Toc326048369 2．在我国光对的化学研究 PAGEREF _Toc326048369 \h 2 HYPERLINK \l _Toc326048370 （二）薄膜在光化学及其他方面中的应用 PAGEREF _Toc326048370 \h 2 HYPERLINK \l _Toc326048371 1．薄膜在抗紫外中的应用 PAGEREF _Toc326048371 \h 3 HYPERLINK \l _Toc326048372 2．在其他方面的应用 PAGEREF _Toc326048372 \h 4 HYPERLINK \l _Toc326048373 （三）纳米薄膜的分类 PAGEREF _Toc326048373 \h 4 HYPERLINK \l _Toc326048374 1．按用途划分 PAGEREF _Toc326048374 \h 4 HYPERLINK \l _Toc326048375 2．按层数划分 PAGEREF _Toc326048375 \h 4 HYPERLINK \l _Toc326048376 3．按微结构划分 PAGEREF _Toc326048376 \h 4 HYPERLINK \l _Toc326048377 4．按组分划分 PAGEREF _Toc326048377 \h 5 HYPERLINK \l _Toc326048378 5．按薄膜的构成与致密度划分 PAGEREF _T