《四氯化钛法制备光催化分离膜及其降解亚甲基蓝的研究》-毕业论文.docVIP

学校代码： 11059 学 号：0803011032 Hefei University 毕业论文 BACHELOR DISSERTATION 论文题目： 四氯化钛法制备光催化分离膜 及其降解亚甲基蓝的研究 学位类别： 工学学士 学科专业： 粉体科学技术与工程 作者姓名： 导师姓名： 完成时间： PAGE I 四氯化钛法制备光催化分离膜及其降解亚甲基蓝的研究 摘 要 光催化降解污水的研究已经有几十年的历史，而且在基础理论和应用方面取得了很多进展，但是距离实现产业化还存在不小的差距，其中主要的问题是缺乏具有良好应用性能的高效光催化剂。本文通过改变各种制备条件，对不同条件下光催化剂对亚甲基蓝降解效果进行研究。 本论文对渗透玻璃膜光催化剂降解亚甲基蓝进行了研究。以四氯化钛为原料，渗透玻璃膜为载体，用溶胶-凝胶法制备出渗透玻璃膜。考察了二氧化钛溶胶浓度、pH值和煅烧温度对渗透玻璃膜光催化剂光催化降解亚甲基蓝的影响，得出当二氧化钛溶胶浓度为0.5mol/L、pH=7和煅烧温度为650℃，亚甲基蓝的最大降解率为5.5%。研究了降解条件对光催化降解染料废水的影响，结果表明：改变溶液浓度、流量和光源等降解条件可以提高光催化剂的催化氧化效果。 关键词：光催化剂；渗透玻璃膜；二氧化钛；溶胶-凝胶；亚甲基蓝 Abstract The use of photo catalytic degradation of wastewater by the method has a history of decades, and in theory and application aspects made a lot of progress, but to achieve industrialization still exist a big gap, the main difficulty is the lack of good application performance of high Dialoguing catalyst. In this paper, the use of self-made experimental device, by changing the preparation conditions, to different light catalyst on degradation effect of ethylene blue. This paper studies photo catalytic degradation methylene blue using permeable glass membrane photo catalyst. The photo catalyst was prepared employing TiCl4 as precursor and permeable glass membrane as support by the sol–gel method. A series photo catalyst was got by varying titanium sol concentration, pH and calcinations temperature. The maximum of degradation rate was for 5.5% phenol when titanium sol concentration is 0.5mol/L, pH=7 and a calcinations temperature was 650 Celsius. The effect of degradation parameters, such as the concentration of solution, velocity of flow and lamp were explored. The results show that the photo catalytic efficiency can be improved by adjusting them. Keywords: Photo catalyst; Permeable Glass Memb