《医学传感器的制作及其测试》-毕业论文.docVIP

武汉工业学院 毕业论文 论文题目：医学传感器的制作及其测试 姓 名： 学 号： 院 系： 化学与环境工程学院 专 业： 材 料 化 学 指 导 教 师： 2012年6月6日 摘要 本实验主要介绍了碳纤维微电极、Ag-AgCl参比电极、Pt微电极的制作与如何使用上述所制得的电极制作医学传感器。近些年来微纳米超微电极在生命科学领域中已取得广泛应用。跟常规电极相比, 微电极有许多显著的性能, 已经广泛应用于分析化学领域与医学生物领域。微电极对材料研究具有比常规尺寸电极更独特的优势。电极的超微尺寸使之能对生物微环境进行实时监测, 还可作为微柱分离的检测器，其使用方面的种种优势在现今的实际生活中得到了广泛的亲睐。本次论文实验也是对医学传感器的一次研究。在实验中我们自制导电胶，用火焰蚀刻法制作碳纤维微电极、Ag-AgCl参比电极、Pt微电极并研制可用于体内监测的医学传感器。对研制的传感电极进行形貌表征和电化学性能测试。测试结果显示研制的医学传感电极具有极低的检测背景电流，背景电流可降低至10 pA；用循环伏安法对多巴胺检测灵敏度低于1.0×10－7 mol/L。测试结果表明该电极具有优良的电化学性质和极高的检测灵敏度，该电极有望成为医学体内监测的强有力工具。 关键词：医学传感电极；碳纤维微电极；火焰蚀刻；检测限 Abstract This study introduces fabrication of the carbon fiber micro- electrode, Ag-AgCl, Pt microelectrode and how to make medical sensors using the above prepared electrode.In recent years, nano-micro electrode in the life sciences has broad applications. Compared with the conventional electrode, microelectrode has many remarkable properties and has been widely used in analytical chemistry and medical biotechnology field. The micro-electrode material is more than unique advantages comparing with the conventional electrode. Ultra small size of the electrode can not only make real-time monitoring of biological micro-environment, but also as the detection in the micro-column separation of make it widely in applied . This experiment also explored the feasibility of a study. Morphological and electrochemical characterization of new sensors has been performed. The result displays very low background current, and even down to a 10-11-ampere level. The detection limit of the new medical sensor for dopamine is less than 1.0×10－7 mol/L by cyclic voltammetry. The results show that the sensor has a very excellent electrochemical behaviors and high sensitivity. It will become a powerful tool for in vivo monitoring from various living tissues and organs. Keywords: Medical sensing electrode; Carbon fiber electrode; Flame etching; Detection limits 目录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc2952613151.引言