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氢化物-原子荧光光谱法测定营养强化剂中总硒含量-食品安全质量
7 5 Vol. 7 No. 5
2016 5 Journal of Food Safety and Quality May , 2016
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*
姜 新 , 刘德晔 , 刘华良
(, 210009)
摘 要: 目的 --方法 -
(4:1, V:V)230 ℃, -;
结果 4.0%, 2.0%
2.0~40.0 ng/mL , 0.9999, 0.028 ng/mL,
93.0%~102.0%, 2.2%(n=6) 结论
,
关键词: ; ; -
Determination of total selenium in selenium nutrition enhancer by refluxing
wet digestion-hydride generation-atomic fluorescence spectrometry
*
JIANG Xin , LIU De-Ye, LIU Hua-Liang
(Jiangsu Provincial Center for Disease Control and Prevention, NanJing 210009, China)
ABSTRACT: Objective To establish a method for the determination of total selenium in nutrition enhancer by
hydride generation-atomic fluorescence spectrometry (HG-AFS) with refluxing wet digestionMethods The nitric
acid-perchloric acid (4:1, V:V) was used as the digestion system with reflux digestion temperature of 230 ℃. Samples
were detected by the method of hydride generation-atomic fluorescence spectrometry. And then the effects of
digestion system, reducing agent and masking agent on fluorescence intensity were investigated. Results The
fluorescence intensity was the strongest using 4.0% hydrochloric acid as acid medium and 2.0% potassium
borohydride. Selenium had a good linear
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