静电纺丝方法制备无机纳米纤维与其性能分析.pdfVIP

Study on the Preparation and Properties of Electrospun Inorganic Nanofibers Abstract Study on the Preparation and Properties of Electrospun Inorganic Nanofibers Abstract One-dimensional nano materials, which have desirable structure and functionalities, have been a subject of recent investigation due to their potential importance. Variety kinds of organic and/or inorganic nanofibers, nanobelts and nanowires have been synthesized and applied. Elelctrospinning technique is a simple and versatile method to prepare continuous ultrafine nanofibers with diameters down to micro and nano scale. Variety kinds of inorganic nanofibers can be prepared by adjusting the ingredient of the spinning solution. The hierarchical nanofibers have high surface area, which have been applied in university laboratories and industry. The nanofibers can be applied in catalysis, sensors, optical devices, filtration and biomedical application. In this paper, inorganic nanofibers were synthesized by sol-gel processing and electrospinning technique, including silica and titania nanofibers. We systematically investigated the parameters which effected the structure of the nanofibers. We also investigated the adsorption property and the photoelectric property of the nanofibers. The results as followed （1） Preparation of silica nanofibers: TEOS and Polystyrene (PS) were added to the PVP solution to prepare spinning solution. PS nanoparticals were incorporated into the silica/PS/PVP nanofibers as the pore-precursors. Hierarchical porous nanofibers with micro-and mesopores were conveniently obtained via the calcination met