放电等离子烧结制备超细晶奥氏体不锈钢的研究.pdf

27 2 Vol. 27, No . 2 2006 6 IRON STEEL VANADIUM TITANIUM June 2006 张 鑫, 刘 静, 李光强 ( , 430081) 304 , 900 e , 30 MPa 50 MPaXRD SEMTEM , 100 ~ 200 nm; , ; , , ; ; ; ; ; TG 142. 71 A 1004- 7638( 2006) 02- 0017- 04 Preparation of Ultrafine Grain Austenitic High- nitrogen Stainless Steel by Spark Plasma Sintering Zhang Xin, Liu Jing, Li Guangqiang ( School of Materials and Metallurgy, Wuh an University of Science and Technology , Wuhan 430081, Hubei, China) Abstract:The SPS ( spark plasma sintering ) process was used to sinter 304 austenitic stainless steel pow der made by milling. The sintering temperature is 900 e , and the sintering stress are 30 MPa and 50 MPa respec- tively. The phase composition and crystallite size of sintered sample w ere analyzed by XRD, SEM and TEM. The results show that the sintered sample matrix is austenite, and the crystallite size is 100 ~ 200 nm approx-i mately . The density of the sample closes to steel, this show the sintering samples attain to high densif icat ion. The rigidity of the samples is higher than that of common austenitic stainless steel. The electrochemistry erosion and metallographic testing show that the more compact the better corrosion resistance of samples is. Key word: spark plasma sintering; densification; electrochemistry erosion ; stainless steel; austenite; powder 大, 因此是制备纳米材料及高致密度细晶粒陶瓷的 0 引言 [ 2]