换热器防垢除垢试验研究-高校化学工程学报.PDFVIP

第23 卷第1 期 高 校 化 学 工 程 学 报 No.1 Vol.23 2009 年 2 月 Journal of Chemical Engineering of Chinese Universities Feb. 2009 文章编号：1003-9015(2009)01-0051-06 换热器防垢除垢实验研究 段培清, 南碎飞, 窦 梅, 徐惠芬, 毛薛刚 (浙江大学 化学工程与生物工程系 化学工程研究所, 浙江 杭州 310027) 摘 要：考察了二甲基甲酰胺中的盐在换热器换热冷却过程中的结垢行为，分别采用内置弹簧和液固流态化以及两者 结合的方法对换热器在线防垢除垢进行研究。采用测定总传热系数法研究污垢热阻随时间的变化规律，并用污垢称重 法测定不同条件的总污垢量。研究了流体流速、传热温差、弹簧结构、惰性固体颗粒数量和大小等诸因素对结垢的影 响，结果表明：直径与管内径比为0.8 ，螺距和管内径比为1.5 的弹簧在0.6~1.0 m⋅s− 1 的流速范围内防垢除垢效果最佳， 随着颗粒数量的增加和粒径的增大，污垢生成速率降低，结垢量减少，相比同条件下单纯颗粒流态化除垢，内置弹簧 和颗粒流态化结合法可以使污垢量减少20%~50% 。实验研究结果对实际的工业过程具有一定的参考意义和指导价值。 关键词：二甲基甲酰胺；防污垢；换热器；液固流态化；内置弹簧 中图分类号：TQ051.5 文献标识码：A Experimental Research on Anti-fouling of Heat Exchanger DUAN Pei-qing, NAN Sui-fei, DOU Mei, XU Hui-fen, MAO Xue-gang (Institute of Chemical Engineering, Department of Chemical and Biochemical Engineering, Zhejiang University, Hangzhou 310027, China) Abstract: The fouling behavior of mixed salts in DMF (N,N-dimethylformamide) solution during cooling in heat exchanger was investigated. The methods of inserting screw spring in the cooling tube, putting solid particles in the cooling tube to form liquid-solid fluidization and the combination of these two measures were adopted respectively to prevent and clean up the fouling scale on the tube wall on-line. The variation of the heat transfer resistance of fouling scale with cooling time was obtained by total heat transfer coefficient method, and the total amount of mixed salts crystallization fouling was measured by weighting method. The effects of fluid ve