液相色谱-串联质谱法检测饲料中26种β受体激动剂类药物残留.PDF

6 4 Vol. 6 No. 4 2015 4 Journal of Food Safety and Quality Apr. , 2015 26 β 2 刘 佳, 梁桂荣, 李少晖，谢云峰, 任丹丹, 杨永坛* (, , 102209) 摘 要: 目的 26 β --(HPLC-MS/MS) 2 方法 , , (MCX)0.1% (A)0.1%-(B), (ESI+)(MRM)β2- 15 min 26 26 β2- 2050 100 μg/L 71.9%~102.9%, 11.8% (n=6), 10 μg/kg , β2- 关键词: β -; -; ; 2 Simultaneous determination of 26 β -agonist residues in feed by liquid 2 chromatography-tandem mass spectrometry * LIU Jia, LIANG Gui-Rong, LI Shao-Hui, XIE Yun-Feng, REN Dan-Dan, YANG Yong-Tan (Beijing Key Laboratory of Nutrition Health and Food Safety, COFCO Nutrition and Health Research Institute, Beijing 102209, China) ABSTRACT: Objective To determination of 26 β -agonist residues in feed samples by liquid chromatography 2 -tandem mass spectrometric (LC–MS/MS). Methods Feed samples were extracted with muriatic acid and methanol solution. And then the β2-agonist residues in the