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3.2.1 供试材料及处理 ·································································13
3.2.2 主要仪器··········································································13
3.2.3 主要试剂··········································································14
3.2.4 试剂的配置·······································································14
3.2.5 怀山药及其零余子样品的制备··············································14
3.2.6 葡萄糖标准曲线的制作 ·······················································14
3.2.7 多糖含量的测定 ·································································15
3.2.8 活性多糖的提取 ·································································15
3.2.9 多糖抗氧化能力的测定························································15
3.3 结果与分析·········································································16
3.3.1 葡萄糖标准曲线·································································16
3.3.2 多糖含量的测定·································································17
3.3.3 多糖抗氧化能力的测定 ·······················································17
3.4 小结··················································································19
第4 章 怀山药零余子尿囊素成分的测定········································20
4.1 引言···················································································20
4.2 材料与方法·········································································20
4.2.1 供试材料及处理 ·································································20
4.2.2 主要仪器···········································································20
4.2.3 主要试剂···········································································20
4.2.4 对照品溶液的制备······························································21
4.2.5 样品溶液的制备·································································21
4.2.6 尿囊素吸收波长的确定························································21
4.2.7 液相色谱条件 ····································································2
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