桂皮精油的提取及其化学成分的GC.pdf

中国农学通报 2012,28(09):264-269 Chinese Agricultural Science Bulletin 桂皮精油的提取及其化学成分的GC-MS 分析 张 艳，仝其根 （北京农学院食品科学学院，北京102206） 摘 要：为比较不同溶剂提取桂皮精油成分的差异性，研究确定了石油醚、正己烷、三氯甲烷3 种溶剂提 取桂皮精油的最佳条件，并对提取的桂皮精油化学成分进行GC-MS 分析比较。结果表明：最佳提取条 件是三氯甲烷为提取溶剂，桂皮和三氯甲烷的比例为1:15(W/V) ，提取时间60 min ，提取3 次；3 种溶剂提 取桂皮精油的化学成分在种类和相对百分含量上呈现差异，但不十分显著。 关键词：桂皮精油；提取；GC-MS 分析 中图分类号：TS202.3 文献标志码：A 论文编号：2011-2858 Extraction and Chemical Composition GC-MS Analysis of Cinnamon Essential Oil Zhang Yan, Tong Qigen (Food Department of Beijing Agricultural College, Beijing 102206) Abstract: To identify the difference of the composition of essential oils extracted using different liquid solvents, cinnamon essential oils were extracted using petroleum ether, n-hexane and chloroform in this study. The optimum extraction condition was found out, and the composition of essential oil was analyzed by using GC-MS. The main conclusions were as follows: the optimum extraction condition was that chloroform was best solvents, cinnamon: chloroform was 1:15 (W/V), extraction time 60 min, extraction count was 3 times; the chemical compositions of essential oils extracted by different extraction liquid solvents in kinds and percentage composition were different, but not significant. Key words: cinnamon essential oil; extracting; GC-MS analysis 0 引言 油树脂是一种成分复杂的芳香精油，经过GC-MS 分 桂皮又称肉桂、官桂或香桂，为樟科植物天竺桂、 析，主要成分是肉桂醛、甲醛、邻甲氧基肉桂醛、δ-杜松 阴香、细叶香桂、肉桂或川桂等树皮的通称。商品桂 油烯、苯丙醛、β-大香叶烯、丁香酚、香豆素、肉桂酸、乙 [10-12] 皮的原植物比较复杂，约有十余种，均为