利用新生相混合氢氧化物吸附处理水溶液中采油用阴离子表面活性剂-环境工程专业论文.docxVIP

山东大学硕士学位论文2．2．11解吸实验 山东大学硕士学位论文 2．2．11解吸实验 21 第三章处理活性石油磺酸盐实验探究 ．22 3．1自泥组分测定 ．．22 3．2吸附前后XRD谱图分析 22 3．3新生相氢氧化物透射电镜照片 23 3．4傅里叶变换红外光谱分析 ．24 3．5溶液pH对吸附效果的影响 25 3．6白泥投加量对吸附效果的影响 27 3．7反应时间及初始石油磺酸盐溶液浓度对吸附效果的影响 ．．29 3．8吸附等温线 ．30 3．9吸附动力学 ．33 3．10热力学参数 36 3．11重金属残留量测定 37 3．12解吸实验 ．．38 3．13本章小结 ．．39 第四章处理木质素磺酸钠实验探究 40 4．1 pH对去除效果的影响 ． ．40 4．2投加量对去除效果的影响 ．40 4．3搅拌时间对去除效果的影响 ．．42 4．4吸附热力学 。43 4．5 FT—IR红外谱图分析 ．．44 4．6本章小结 46 第五章结论与展望 ． ．47 5．1结论 ．47 5．2展望 ．48 参考文献 ．．49 致谢 ． ．．55 攻读学位期间发表的学术论文 ．．56 II 万方数据 山东大学硕士学位论文Content 山东大学硕士学位论文 Content Abstract in Chinese ．．1 Abstract in English ．．． ． ．．．．． ．．．． ．．．．．．． ．．．．．．．．．．3 1．Instruction 5 1．1 Suffactant wastewater 5 1．1．1 Surfactant 5 1．1．2 Surfactantwastewater ．．7 1．2 Tbatment ofsurfactant wastewater 7 1．3 Co-precipitate／Adsorption 。l l 1．4 The white mud 12 1．5 Background and contents ofresearch ．13 1．5．1 Background ofresearch 13 1．5．2 The contents of research ．．14 2 Methods and materials ． ．． ． ．． ． ． ． ．16 2．1 Chemical reagents and equipment 16 2．1．1 Chemical reagents 16 2．1．2 Experimental equipment ．．16 2．2 Methods ．．17 2．2．1 Preparation ofthe leaching solution ofwhite mud ．17 2．2．2 Determination of the solid content of the white mud leaching solution 17 2．2．3 Determination of the mass of freshly generated hydroxide precipitates 17 2．2．4 Separation ofpetroleum sulfonate surfactant components ．18 2．2。5 Analytical method and standard curve ．．19 2．2．6 Preparation ofusing solution ．19 2．2．7 Adsorption experiments 20 2．2．8 Characterization of white mud and freshly generated hydroxide precipitates ．．：!() I 万方数据 山东大学硕士学位论文2．2．9 山东大学硕士学位论文 2．2．9 XRD analysis ofprecipitates before and after adsorption ．．20 2．2．10 FT-IR analysis ofprecipitates before and afteradsorption ．．21 2．2．11 Desorption experiments ·21 3 Removal ofpetroleum sulfonate by freshly generated hydroxide precipitates 22 3．1 The chemical composition ofthe white mud 一22 3．2 XRD analysis． ．．