非晶态Cu2fZnO-Al2O3催化剂上甲醇和二氧化碳合成碳酸二甲酯.pdfVIP

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非晶态Cu2fZnO-Al2O3催化剂上甲醇和二氧化碳合成碳酸二甲酯.pdf

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目录目录摘要································································································I Abstract ······························································································II 第1 章绪论 ························································································1 1.1 引言···························································································1 1.2 碳酸二甲酯的性质 ········································································1 1.3 碳酸二甲酯的用途 ········································································2 1.3.1 用作羰基化试剂来代替光气························································2 1.3.2 用作甲基化试剂来代替硫酸二甲酯···············································2 1.3.3 用作绿色溶剂··········································································2 1.3.4 用作油品添加剂·······································································3 1.4 DMC 的合成方法···········································································3 1.4.1 光气法···················································································3 1.4.2 甲醇氧化羰基化法····································································3 1.4.3 亚硝酸钾酯的羰基化法······························································4 1.4.4 酯交换法················································································4 1.4.5 甲醇和CO2 合成DMC 法···························································4 1.5 试验的前期工作 ···········································································9 1.6 本文研究的内容 ·········································································10 第2 章实验部分················································································11 2.1 仪器与试剂················································································11 2.1.1