凝胶渗透色谱-食品安全质量检测学报.pdf

6 3 Vol. 6 No. 3 2015 3 Journal of Food Safety and Quality Mar. , 2015 17 * 何曼莉, 谢建军 , 陈 捷, 卢 丽, 陈文锐 (, 510623) 摘 要: 目的 (gel permeation chromatography, GPC)(solid phase extraction, SPE)( ), , , , , , 17 方法 , (1:1, v:v), , , ( µECD )结果 17 10~100 µg/kg , R0.999, , 17 84.6%~115.5%, (RSD, n=6) 3.1%~14.5% (LOQ) 0.31~4.15 µg/kg结论 , 17 关键词: ; ; ; ; Determination of 17 organochlorine pesticide residues in traditional Chinese medicinal herbs by gel permeation chromatography-solid phase extraction-gas chromatography method * HE Man-Li, XIE Jian-Jun , CHEN Jie , LU Li, CHEN Wen-Rui (Guangdong Entry-Exit Inspection and Quarantine Bureau, Guangzhou 510623, China) ABSTRACT: Objective To establish an analytical method for detecting hexachlorocyclohexane, dichlorodiphenyltrichloroethane, endosulfan, heptachlor, chlordane, aldrin, dieldrin, endrin and their metabolites residues in traditional Chinese medicinal herbs including plumeria, dried date, ginseng, dangshen, radix ginseng rubra, cordate houttuynia and astragalus with gel permeation chromatography-solid phase extraction-gas chromatography method. Methods Tr