《以蛋壳为原料制备乳酸钙论文》-毕业设计（论文）.docVIP

PAGE l 四川理工学院毕业论文 第2章材料与方法 四川理工学院毕业论文 以蛋壳为原料制备乳酸钙 学 生： 学 号： 专 业：化学工程与工艺 班 级：工艺 指导老师： 四川理工学院材料与化学工程学院 年 六 月 四川理工学院毕业论文 以蛋壳为原料制备乳酸钙 - PAGE I - 摘 要 四川理工学院本科毕业论文 摘 要 - PAGE I - 本论文先采用直接中和法以验证蛋壳为原料制备乳酸钙的可行性，然后将蛋壳进行预处理后，加入乳酸进行中和反应制备乳酸钙。先采用单因素实验，对影响乳酸钙收率的各个因素进行了初步研究，得出最佳单因素工艺条件；在此基础上进行了正交试验研究，并对试验结果进行极差和方差分析，确定了优化工艺条件。试验结果表明：影响乳酸钙提取效果的因素顺序为料液比反应温度反应时间加水量；当加入蛋壳粉用量与乳酸用量料液比1：1.6，蒸馏水用量为 80mL，在中和反应温度35℃、反应时间 1.5h的条件下，乳酸钙的产率可达 91.34%，质量分数达到 90.93%。 关键词：蛋壳；直接中和法；乳酸钙；产率 四川理工学院毕业论文 以蛋壳为原料制备乳酸钙 - PAGE II - Abstract ? As we know, it has so many active ingredient in eggshell but it has not been used as materials of industries, we should try our best to make fully use of these ingredients, it can not only improve economic benefit , but also can reduce the pollution of the environment. caused by the eggshell .?in this paper, calcium lactate was made from eggshell. The eggshell was fully utilized, we added the lactate to react with eggshell to make calcium lactate by direct reaction. We used a single-factor approach, then we chosed the optimal reaction condition. The results of experiment were analyzed by significance analysis. The results showed that the optimum conditions were: adding solid-liquid ratio 1:1.6. distilled water 80 mL, and the reaction temperature 35℃, reaction time 1.5h, The results showed the yield of calcium lactate can reach 91.34% and the content was 90.93%. Key words: eggshell；direct reaction；calcium Lactate；yield 四川理工学院毕业论文 以蛋壳为原料制备乳酸钙 - PAGE ii - 目 录 TOC \o 1-3 \f \h \u 摘 要