废水中悬浮物测定(英文版).docVIP

ExperimentⅠthe determination of suspended solid in wastewater The purpose and requirements of the experiment Learn the method of the determination about suspended solid (call SS hereinafter); Review the usage of analytical balance and the error about operation; Know the mean of washing residuum in filter; Know SS’s the danger and the relative with turbidity; Experimental program Experimental instruments and drugs Filter paper and funnel; Analytical balance and weighing bottle; Drying oven; Water of Yellow River. Experimental steps Oven dry and weigh before filter: chill weighing bottle after take out from drying oven. Then weigh weighing bottle twice with folded filter paper, recording the data, and the D-value between two times must less than 0.2mg. Filtering and oven dry: take Yellow River water 50mL, 50mL, 100mL, with mixing. Then respectively filter them and washing water of the beaker. After filtering, wash the residuum three times in funnel. Ultimately take filter and remains into weighing bottle, and oven dry them 1.5 hours with 104℃ in drying oven. Weighing: when weighing bottle and remains have cooled, weigh them, recording the data, and the D-value between two times must less than 0.2mg. Experimental result and data handling The data about SS 　 Weight after the first oven dry(g) Weight after the second oven dry(g) Residuum(g) mass concentration of SS (mg/L) 50mL water 43.1356 43.1253 43.2112 43.2106 0.0805 1610 50mL water 44.0954 44.0959 44.1732 44.1739 0.0779 1558 100mL water 43.5862 43.5858 43.7987 43.7993 0.2130 2130 According to following formula we can calculate the mass concentration of SS in Yellow River. Notes: mA refers to the mass of residuum + filter paper and weigh bottle (g) mB refers to the mass filter paper and weigh bottle (g) V refers to the volume of water sample (mL) Conclusion Data reliability analysis The average of the mass concentration The standard deviation of the mass concentration The relative standard deviation