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7.3.18 Table 999.04B Results of interlaboratory study for HCB
AOAC Official Method 999.04
TC WG WP SC
Determination of Chlorothalonil
No. of labs 8 8 9 8
and Hexachlorobenzene
in Technical and Formulated Materials Mean (wt %) 0.0201 0.0376 0.0210 0.0185
Capillary Gas Chromatography sr 0.0007 0.0019 0.0010 0.0006
First Action 1999 sR 0.0012 0.0021 0.0045 0.0010
RSD , % 3.5 5.0 4.8 3.4
[This method is applicable to analysis of technical material (TC), dry r
formulations (WP and WG), and aqueous-based (SC) formulations RSD , % 6.0 5.5 21.6 5.4
R
from 50 to 99% chlorothalonil (CTL) and 0.01 to 0.1% hexachloro- For TC, WG, and SC, one laboratory was identified as an outlier by the single
benzene (HCB).] Grubb’s test. For WP, no outlier tests were significant.
See Tables 999.04A and B for the results of the interlaboratory
study supporting acceptance of the method.
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