放大染色胃镜下氩气刀治疗胃黏膜隆起糜烂的临床研究.docxVIP

放大染色胃镜下氧气刀治疗胃黏膜 隆起糜烂的临床研究 【摘要】目的建立反相高效液相色谱 法测定奥扎格雷的含量。采用Kromasil C18 (x 150mm, 5m)色谱柱以/L磷酸二氢钾- 乙月青为流动相，流速为/min ,以左羟丙哌嗪 为内标物，检测波长为274nm结果奥扎格 雷的回归方程Y=+(r=),其线性范围为? 416 [I g/ml ,平均回收率为 ％结论 本法可 用于奥扎格雷的含量测定，操作简便，结果 准确。 【关键词】反相高效液相色谱法；奥扎格 雷；含量测定 Abstract: Objective To develop a RP-HPLC procedure in determination the quantity of ozagrel. Methods HPLC was carried out using a Kromasil C18 column (x 150mm, 5 从 m) with /L Potassium dihydrogen phosphate()-acetonitrile (85 : 15) as the mobile phase, the flow rate was /min, the internal standard was levodropropzine. The UV wavelength was 274nm. Results The