实训基地 校外实训基地 哈克流变仪在聚合物加工和表征方面的应用——Melt Flow Tester.pptVIP

* Haake Melt Flow Tester MFR = Mass of a polymer sample Pressed by a standardized weight Through a die with a standardized geometry In a standardized time ( 10 minutes ) At standardized conditions Unit: [g/10min] What is Melt Flow Rate ? Principle design of a Melt Flow Rate tester d = 2,095 ± 0,005 mm L = 8 ± 0,25 mm Die: Cutter Heated measuring chamber Measuring cylinder ( D = 9.55 mm ) Sample Thermal insulation Measuring piston Weight MVR = Unit: [ccm/10min] What is Melt Volume Rate ? Volume of a polymer sample Pressed by a standardized weight Through a die with a standardized geometry In a standardized time ( 10 minutes ) At standardized conditions Principle design of a Melt Volume Rate tester d = 2,095 ± 0,005 mm L = 8 ± 0,25 mm Die: Length measuring system Heated measuring chamber Sample Thermal insulation Measuring piston Weight Measuring cylinder ( D = 9.55 mm ) Length measuring systems Optical systems: Simple light barrier: Reflexion light barrier : Incremental length measuring systems : Detectionmethodes: Optical Mechanical Magnetical Elektrical Length measuring systems Meltdensity – f(T) Testconditions ISO1133 Material DIN 53735 ISO 1133 ASTM 1238 Temp. [°C] Load [kg] ASA U 9 - 220 10,00 PC W 21 - 300 1,20 PET S 17 - 280 2,16 PBT A 1 - 250 2,16 PMMA N 13 I 230 3,80 PB D F 4 6 E N 190 2,16 10,00 POM D 4 E 190 2,16 Material DIN 53735 ISO 1133 ASTM 1238 Temp. [°C] Load [kg] PS H 8 G 200 5,00 PE D G T 4 7 5 E F P 190 2,16 21,6 5,00 PP M 12 L 230 2,16 ABS U 9 - 220 10,00 E/VAC B D Z 2 4 22 C D Z 150 190 125 2,16 2,16 0,325 SAN U 9 - 220 10,00 Testconditions ISO1133 Viscosity Functions of PP with different MFR values A 1.6 B 3.3 C 13.0 D 24.8 E 32.4 MFR (230/2.16) PP- 230°C 100 101 101 102 103 104 102 103 104 Shear Rate [1/s] Viscosity [Pas] Melt Flow Rate Weight [kg] 0,325 1,2 2,16 3,8 5 10 15 21,6 Shear Stress [Pa] 2956 10920 19650 34570 45480 90960 136400 196500 MFR [g/10min] 0,5 1 1,5 3 5 8 10 25 Shear Rate [1/sec] 0,92