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工业循环水水质分析操作规程.docx

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工业循环水水质分析操作规程 ———————————————————————————————— 作者： ———————————————————————————————— 日期：水质分析操作规程江苏江海化工集团有限公司 2008 年 12 月目录 1．0 目的 ··············································· (4) .0 适用范围 ···········································（ 4) ０管理要求··········································· (4) 4.0 职责···············································（ 4）５.0 作业前准备 ·········································(4 ） 6.0 水质分析工作流程· ·································· (4) 7.0 水质分析方法一般规定 ·······························( ４) 8．0 水质分析方法 ······································· (5) 8.1 PH 值的测定（电位法 ) ······························（ 5) 8.2 电导率的测定（电导仪法 ) ····························(8 ） 8.3 浊度的测定（浊度仪器法） ····························（1１） 8． 4 悬浮物的测定（重量法 ) ······························( １3) 8．5 总硬度的测定 (EＤTA络合滴定法 ) ······················（14) ６钙离子的测定（ EDＴＡ络合滴定法）·····················（１ 7) A 按中石化法······································· (17 ）按国标法·········································(1 ８) 8.7 总碱度的测定（指示剂法） ····························（２ 0) 按国标法·········································（ 20）按中石化法·······································（22）８氯离子的测定······································（２ 5) 甲硝酸银滴定法···································( ２5) 乙硝酸汞滴定法···································（２ 6）８.9 铁离子的测定 ( 邻菲罗啉分光光度法 ) ················· (28 ）１ 0 总磷的测定（钼酸铵分光光度法 ) ····················（3０) A 法········································（3０) B 法·······································(32 ） 8.11 游离氯和总氯的测定（ DPＧ分光光度法）···············（３ 9) 8．12 锌离子的测定（ EＤＴ A 络合滴定法）····················（43）１3 硫酸根的测定 (EＤTA 滴定法）························（４ 5) 8.14 铜离子的测定 ( 二乙基二硫代氨基甲酸钠分光光度法） ··（ 4８ ) 8.15 硫化物的测定 ( 亚甲基兰分光光度法 ) ················（51) １6 油含量的测定（红外油分分析仪法 ) ··················( ５3) 8．1７氨氮的测定（纳氏试剂比色法） ·······················(55) 8.1 ８异养菌的测定 ( 标准平皿计数法 ) ····················（57） 8.19 C ＯＤ化学需氧量的测定（重铬酸钾法 ) ·················（６ 2） 8.20 二氧化硅的测定（硅钼黄还原分光光度法） ············（64）８． 2１硝酸根的测定（ 2,6- 二甲基苯酚分光光度法） ·········（