基于回复与再结晶的退火1介绍.pptx

第四章 基于回复与再结晶 过程的退火 (1);（1) 对象:冷变形或有严重内应力的金属及其合金;（4) 退火过程中主要固态转变:;冷变形金属 (1)纤维组织 (2)变形织构 (3)晶格畸变（储能） (4)晶体缺陷（储能）：点缺陷、位错、亚晶界、堆垛层错等以及位错缠结、位错网胞等亚结构;Al with high purity compressed (strain of 0.3). Polycrystal specimen. ;SEM backscattered micrographs of large-grained Al-0.1Mg: (a) deformed 50%, showing cell bands aligned at ?40o to rolling plane, (b) deformed 70%, showing large scale deformation banding of grain A. ;EBSD maps for microstructure of medium-sized Al-0.1Mg after deformation at strains: (a) 0.69, (b) 1.2, (c) 2.6, (d) 3.9. Comparison with large-sized materials, here the low angle boundaries are less aligned, and new high angle boundaries through deformation banding is less extensive and tends to occur mainly at the higher strains.;Optical micrograph of the as-cast AA5754 alloy cold rolled to 95% reduction showing the alignment of particles and particle clusters (arrows) on the longitudinal plane along the rolling direction.;在加热退火过程中组织变化：冷变形储能使冷变形金属的自由能提高，这是加热过程中组织变化的驱动力。经回复、再结晶、晶粒长大等过程，完全再结晶的金属组织和性能恢复到平衡态。不完全的可能停留在中间阶段。;Pure Ag deformed 50% and annealed at 300OC for 30S. Longitudinal, compression, shear bands, recrystallization;Summary: Upon annealing after cold deformation ;TEM images showing a tendency of cell formation of the AA5182 strained to 2.4.;Metal with lower energy of stacking fault: Early stages of recrystallization: Observations were carried out on the longitudinal section within the shear band area of a Ag crystal deformed 67% and annealed at 265C for 30S.;冷变形33%;Discontinuous recrystallization in large-grained Al-0.1Mg (a) and AA8006 (b) at strain 3.9 annealed for 1 hour at 250oC.;;原位再结晶与再结晶区别： （1）小角度晶界（小于10~15o）与大角度晶界 （2）退火织构仍与原变形织构相同 原位再结晶实际上是指在一定的条件下，随着温度升高，时间延长，亚晶长大到相当大（如大于10μm），晶体取向几乎保持不变，而并形成新的再结晶晶核。 原位再结晶是多边化和胞状亚组织形成的亚晶通过亚晶界迁移和亚晶粒合并的方式逐渐粗化后进一步长大粗化的过程。 而这种亚晶进一步粗化实际上仍处于亚晶粗大化范畴，不是真正意义上的再结晶。;加热退火过程中性能变化：;4. 3 回复退火;1——层错能低，如Cu、Ni、Ag、γ-Fe等及其合金 点缺陷动，而位错不变，物理、化学性能变化明显，而力学性能基本不下降，加工硬化几乎完全保留，甚至有的合金还有所升高（低温退火硬化）； 2——层错能中，