年产2万吨废润滑油回收装置溶剂萃取系统设计.docxVIP

2万吨/年废润滑油回收装置溶剂萃取系统设计 摘 要 溶剂萃取是化工生产中的重要环节，在化工生产中常使用塔设备对混合物进行分离提纯。本设计运用筛板塔和浮阀塔对废润滑油进行萃取分离，经过对比分析丙烷、糠醇、NMP的萃取效果，选择丙烷作为萃取剂，原理是废润滑油中的组分在丙烷中的溶解度不同，经过沉降塔逆流萃取塔顶采出脱沥青油（DAO），塔釜采出脱油沥青（DOA），在分别进行精馏回收萃取剂丙烷。 本文设计了废润滑油以丙烷为溶剂的萃取工艺流程，首先进行了溶剂的对比和选取，然后对质塔设备的物料衡算、能量衡算、主要设备的工艺尺寸进行计算，并选定了适合的附属设备，绘制出PFD图和PID图。 关键词：废润滑油；丙烷；溶剂萃取系统 Design of solvent extraction system for 20000 t / a waste lubricating oil recovery unit Abstract Solvent extraction is an important part of chemical production. In chemical production, tower equipment is often used to separate and purify the mixture. This design uses sieve plate tower and float valve tower to extract and separate the waste lubricating oil. After comparative analysis of the extraction effect of propane, furfuryl alcohol and NMP, propane is selected as the extraction agent. The principle is that the components in the waste lubricating oil have different solubility in propane. The deasphalted oil (DAO) is extracted from the top of the countercurrent extraction tower of the settling tower, and DEA is extracted from the bottom of the tower. The deasphalted oil (DOA) is respectively rectified and recycled Collect the extractant propane. In this paper, the extraction process of waste lubricating oil with propane as solvent is designed. Firstly, the solvent is compared and selected. Then, the material balance, energy balance and process size of main equipment of the quality tower are calculated, and the appropriate auxiliary equipment is selected PFD Figure and PID Figure. Keywords: waste lubricating oil; Propane; solvent extraction system 目 录 TOC \o 1-3 \h \z \u 1 前言 1 1.1研究背景 1 1.2研究意义 1 2 生产工艺 2 2.1废润滑油萃取溶剂 2 2.1.1丙烷萃取 2 2.1.2糠醇萃取 2 2.1.3NMP萃取 2 2.2废润滑油生产工艺 3 2.3丙烷溶剂萃取系统 3 3工艺计算 5 3.1物料衡算 5 3.1.1衡算依据 5 3.1.2衡算过程 6 3.2能量衡算 17 3.2.1衡算依据 17 3.2.2衡算过程 18 4设备选型 19 4.1设备的选型及原则 19 4.1.1塔设备的选型及原则 19 4.1.2换热器的选型及原则 19 4.1.3机泵的选型及原则 20 4.1.4压缩机的选型及原则 21 4.1.5储罐的选型及原则 22 4.2主要设备选型计算