HAPSITEER高级操作培训.pptxVIP

HAPSITEER高级操作培训第1页/共182页第2页/共182页Instrument Setup仪器设置Insert Gas Canisters 插入气瓶 Turn on the Analytical Module or take the Analytical Module out of Extended Standby将分析模件电源 on 或将分析模件离开延伸的待机状态System will heat, AutoTune and run a Concentrator cleanout 系统将加热, 自动调谐和运行浓缩器清理Turn on the Laptop 将计算机电源 onDouble click the ER IQ/Plus IQ icon to open the software 双击 ER IQ/Plus IQ 图标, 打开软件 第3页/共182页Tune调谐Tune Overview 调谐概述AutoTune自动调谐Manual Tune手动调谐第4页/共182页Tune Overview调谐概述Tune optimizes the performance of the MS调谐使 MS 的性能最佳化An improperly tuned MS can result in:未正确调谐的 MS 可导致:Low sensitivity 灵敏度低Undetected compounds未能检测到化合物Mass misalignment质量数未对准Incorrect identifications不正确的 ID 鉴别Incorrect Mass Ratios不正确的质量比Low Net Fit or SI numbers低纯拟合或 SI 数第5页/共182页Tune Overview调谐概述Ten masses are used when tuning the MS调谐 MS 使用 10 个质量数Masses are between 50-282 to encompass the full 41-300 range of mass fragments质量数在 50-282 之间包含整个 41-300 质量分裂物范围The Internal Standard gas contains the chemicals that provide these masses used for tuning内部标准气体包含提供这些用于调谐质量数的化合物第6页/共182页AutoTune 自动调谐The HAPSITE will automatically AutoTune: HAPSITE 将自动调谐:Upon Startup 当启动时Upon exiting Extended Standby当退出延伸的待机状态时After 12 hours of operation运行 12 个小时后第7页/共182页AutoTune自动调谐AutoTune can be initialized by:自动调谐可由下列动作起始 :Clicking Tune AutoTune on the laptop在计算机上单击 Tune AutoTuneTouching RUN AUTOTUNE on the front panel触摸面板上的 RUN AUTOTUNE 按钮Rebooting the HAPSITE重新启动 HAPSITE第8页/共182页Troubleshooting a Failed AutoTune不成功自动调谐的故障查找Internal Standard Canister内部标准气瓶 Verify that the pressure is adequate 核实压强是否适当Verify the expiration date 核实是否已到使用期限Insert new IS canister if necessary 必要时插入新的 IS 气瓶Carrier Gas (Smart Plus Only) 载气 (仅 Smart Plus) Verify pressure that the pressure is adequate 核实压强是否适当Reservoir pressure ( 400 kPa) 贮存器压强 ( 400 仟帕) ER does not have a reservoir ER 无贮存器Insert new Carrier Gas canister if necessary必要时插入新的载气瓶Repeat AutoTune 重新执行自动调谐第9页/共182页Tune Requires Advanced Mode 调谐要求高级模式 The Access Level must be set to