不同形貌纳米四氧化三钴的液相合成表征及性能研究的中期报告.docxVIP

不同形貌纳米四氧化三钴的液相合成表征及性能研究的中期报告 摘要： 本中期报告主要介绍了不同形貌的纳米四氧化三钴（Co3O4）通过液相合成法制备的方法以及其表征和性能研究。通过调控合成条件，分别得到了纳米棒、纳米球和纳米片三种形貌的Co3O4，利用X射线衍射（XRD）、透射电镜（TEM）、高分辨透射电镜（HRTEM）、扫描电子显微镜（SEM）等手段对其进行了表征。实验结果表明，不同形貌的Co3O4添加到锂离子电池负极材料中，可以有效改善其循环性能和倍率性能。 关键词：纳米四氧化三钴；液相合成；形貌；表征；性能研究；锂离子电池 Abstract： This midterm report mainly introduces the preparation, characterization and performance study of different morphologies of nanosized Co3O4 by liquid phase synthesis. Nano rods, nano spheres and nano plates of Co3O4 were obtained by adjusting the synthesis conditions, and their structures were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM) and scanning electron microscopy (SEM). The experimental results showed that different morphologies of Co3O4 added to the negative electrode material of lithium-ion batteries can effectively improve their cycling performance and rate performance. Keywords: Co3O4; liquid phase synthesis; morphology; characterization; performance study; lithium-ion battery.