锂离子电池新型正极材料磷酸铁锂的制备与改性研究的中期报告.docxVIP

锂离子电池新型正极材料磷酸铁锂的制备与改性研究的中期报告 摘要： 磷酸铁锂是一种新型的正极材料，具有较高的比容量和长寿命的特点，被广泛应用于锂离子电池领域。本研究以新型的磷酸铁锂为对象，对其制备方法进行了研究，并对其进行表面改性，以提高其电化学性能和循环寿命。首先，采用溶胶-凝胶法制备出磷酸铁锂前驱体，然后采用固相反应法对其进行进一步烧结，制备出磷酸铁锂颗粒。在此基础上，利用化学溶液法和高温碳热还原法对其进行表面改性。通过扫描电镜、X射线衍射、电化学测试等方法对其进行了表征和分析。结果表明，改性后的磷酸铁锂具有更好的结晶性、电化学性能和循环寿命，具有更好的应用前景。 关键词：磷酸铁锂；制备；改性；锂离子电池；电化学性能 Abstract: Lithium iron phosphate is a new type of cathode material with high specific energy and long cycle life, which has been widely used in the field of lithium-ion batteries. In this study, a new type of lithium iron phosphate was used as the object, and its preparation method was studied. The surface modification was carried out to improve its electrochemical performance and cycle life. Firstly, lithium iron phosphate precursor was prepared by sol-gel method, and then further sintered by solid state reaction to prepare lithium iron phosphate particles. On this basis, chemical solution method and high temperature carbon thermal reduction method were used to modify its surface. The characterization and analysis of scanning electron microscopy, X-ray diffraction, electrochemical test were carried out. The results showed that the modified lithium iron phosphate had better crystallinity, electrochemical properties and cycle life, and had better application prospect. Keywords: lithium iron phosphate; preparation; modification; lithium ion battery; electrochemical performance