ASTM E475-16美国材料与试验协会标准.pdfVIP

Designation:E475−16

StandardTestMethodfor

AssayofDi-tert-ButylPeroxideUsingGasChromatography1

ThisstandardisissuedunderthefixeddesignationE475;thenumberimmediatelyfollowingthedesignationindicatestheyearof

originaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.A

superscriptepsilon(´)indicatesaneditorialchangesincethelastrevisionorreapproval.

1.Scope*areasaremeasured.Theconcentrationofdi-tert-butylperoxide

1.1Thistestmethodcoverstheassayofdi-tert-butylisdeterminedbyareanormalizationaftercorrectingforthe

peroxideusinggaschromatography.Itisapplicabletocom-areaofthesolventpeak.Theassayofdi-tert-butylperoxideis

mercialdi-tert-butylperoxidewhichmaycontainsmallcorrectedforwater,whichisdeterminedusingaseparateKarl

amountsofisobutylene,tert-butanol,tert-butylhydroperoxide,Fischertitrationsincewaterisnotdetectedusingflame

triisobutylenes,andwaterasimpurities.ionizationdetection.Theareapercentofdi-tert-butylperoxide

isassumedtobeequaltomasspercent.

1.2ThevaluesstatedinSIunitsaretoberegardedas

standard.Nootherunitsofmeasurementareincludedinthis5.SignificanceandUse

standard.

5.1Di-tert-butylperoxideiswidelyusedasacatalystand

1.3Thisstandarddoesnot