ASTM E463-14a美国材料与试验协会标准.pdfVIP

Designation:E463−14a

StandardTestMethodfor

DeterminationofSilicainFluorsparbySilico-Molybdate

VisibleSpectrophotometry1

ThisstandardisissuedunderthefixeddesignationE463;thenumberimmediatelyfollowingthedesignationindicatestheyearof

originaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.A

superscriptepsilon(´)indicatesaneditorialchangesincethelastrevisionorreapproval.

1.Scopephotometricallyafterextractionofthesilico-molybdatecom-

1.1Thistestmethodcoversthedeterminationofsilicainplexwithnormalbutylalcohol.Photometricmeasurementof

fluorsparinconcentrationsfrom0.5%to10%.theextractismadeat400nm.

1.2ThevaluesstatedinSIunitsaretoberegardedas5.SignificanceandUse

standard.Nootherunitsofmeasurementareincludedinthis

5.1Thistestmethodisintendedasarefereemethodfor

standard.

compliancewithcompositionalspecificationsforimpurity

1.3Thisstandarddoesnotpurporttoaddressallofthecontent.Itisassumedthatallwhousethisprocedurewillbe

safetyconcerns,ifany,associatedwithitsuse.Itisthetrainedanalystscapableofperformingcommonlaboratory

responsibilityoftheuserofthisstandardtoestablishappro-practicesskillfullyandsafely.Itisexpectedthatworkwillbe

priatesafety