现代有机质谱概论课件.pptxVIP

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现代有机质谱概论课件.pptx

现代有机质谱概论

ModernOrganicMassSpectrometry(OMS)MolecularMassSpectrometry

OMSisabasicandhigh-technicalscience.Inwhich,physics,electronicsandcomputersciencewereappliedtostudyphysicalandchemicalcharacteroforganicmolecules

MassSpectrometryhaditsorigininearlylastcenturyApplicationoforganicmassspectrometryforchemicalanalysisoccurredinearly1940s

Quantitativeanalysisofhydrocarbonmixtures(9)producedincatalyticcrackersMethodsrequiretimeFractionaldistillation,refractiveindex200hoursOrganicmassspectrometryonehourormore

Beginninginthe1950s,chemistshaveusedcommercialorganicmassspectrometerforidentificationandstructuralelucidationofawidevarietyoforganiccompounds

TheuseoftheMScombinedwiththeNMRIRandUVrevolutionizedthewayorganicchemistswentaboutidentifyinganddeterminingthestructureoforganicmolecules

MassSpectrometryDeterminemolecularweightElucidatestructureoforganicmoleculeIdentifyunknowncompoundsQuantifyknownmaterialsAccuracy,sensitiveandrapid

OMShasbeenapowerfulanalyticaltoolinmodernstructurechemistryandanalyticalchemistry

Beforethemiddleofthe1970sOMScouldonlyanalyzeorganicmoleculeswithmolecularweightbelow1000Da

1974PlasmaDesorptionMassSpectrometryPD-MS1981FastAtomBombardmentMassSpectrometryFAB-MS1988ElectrosprayIonizationMassSpectrometryESI-MS1988Matrix-assistedLaserDesorptionIoniz

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