粗晶DT4纯铁晶粒细化工艺研究.pdfVIP

HotWorkingTechnolog2019,Vol.48,No.5

粗晶DT4纯铁晶粒细化工艺研究

江学强，吉卫，曹海桥，范啟超

(中国工程物理研究院机械制造工艺研究所，四川绵阳621900)

摘要：纯铁晶粒一般非常大，通过大塑性变形后加热到再结晶温度可以实现晶粒细化。通过室温自由锻和等通道

挤压(ECAP)实现了DT4纯铁的大塑性变形，将粗大不均匀晶粒破碎成微细亚结构，再经完全再结晶处理使DT4晶粒

细化，晶粒度由原材料1级(晶粒直径约254“n)细化至8.5级(约18.9pm)。力学性能研究表明，细晶纯铁力学性能与

粗晶纯铁的接近，晶粒细化对纯铁强化作用不明显。

关键词：粗晶纯铁；冷变形；晶粒细化

DOI:10.14158/j.cnki.1001-3814.2019.05.022

中图分类号:TG306文献标识码：A文章编号:1001-3814(2019)05-0088-05

StudyonGrainRefinementProcessofCoarseGraineDT4PureIron

JIANGXueqiang,JIWei,CAOHaiqiao,FANQichao

(InstituteofMechanicalManufacturingTechnology,ChinaAcademofEngineeringPhysics,Mianyang621900,China)

Abstract:Thegrainsizeofpureironisusuallverlarge.Grainrefinementcanberealizedblargeplasticdeformation

andthenheatingtorecrystallizationtemperature.LargeplasticdeformationofDT4pureironwasrealizedbroom

temperaturefreeforgingandequalchannelangularpressing(ECAP).Thecoarseandinhomogeneousgrainswerebrokeninto

finesubstructures,andthentheDT4grainswererefinedbcompleterecrystallization.ThegrainsizeofDT4wasrefinedfrom

grade1(graindiameterabout254|xm)ofrawmaterialtograde8.5(about19|xm).Thestudofmechanicalproperties

showsthatthemechanicalpropertiesofthefinegrainpureironareclosetothoseofthecoarsegrainpureiron,andtheeffect

ofgrainrefinementonthestrengtheningofthepureironisnotobvious.

Keywords:coarsegrainpureiron;colddeformation;grainrefinement

固态金属晶粒细化的方法主要有两种：一种通来实现晶粒细化。

过热处理来细化晶粒，包括形变热处理工艺和快速

1纯铁试样制备

加热冷却循环工艺，主要适用于有相变金属的晶粒

细化［1］；另一种是剧烈塑性变形法(severeplastic