石墨烯-铜复合粉体制备工艺研究.docxVIP

HotWorkingTechnology2019,Vol.48,No.82 1 21

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???：???；???-?????；XRD；SEMDOI:10.14158/j.cnki.1001-3814.2019.08.031

?????：TB333.1+2 ?????：A ????：1001-3814(2019)08-0128-04

StudyonPreparationProcessofGraphene-copperCompositePowderZHANGHui,GUANTong

(SchoolofMaterialsScienceandEngineering,ShaanxiUniversityofTechnology,Hanzhong723001,China)Abstract：Byusinggrapheneoxideandcoppersulfateasrawmaterials,hydrazinehydrateasreducingagent,the

graphene-coppernano-powderaspreparedaftercentrifugationanddryingbychemicalreductionmethod.Thegraphene/coppercompositenano-powderswerepreparedbysinglevariablemethod,thatis,grapheneoxideasquantificationandcoppersulfateasvariable.TheresultsofXRD,SEMcharacterizationshowthat,whenthemassratioofgrapheneoxidetocoppersulfateis1∶4,thegrapheneandnano-copperinthemixedpowderarethebest.TheCuareparticlesdistributeduniformlyaroundthegraphenelayer.

Keywords：graphene;graphene-coppernanopowder;XRD;SEM

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?，???????????????????，???????????????[2-4]。????????????26.521m2/g，??????????????????。????????????135GPa，????????100??。???????????????????，???????

?CNT（????）??，??1000GPa??[5-8]。

?????????，?????????????????????，???????????????，???????，?????-?????。??XRD（λ=0.1541841nm，?????20mA，?????40kV）?????????。??????????40°～80°，?????10（°）/min。?

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????:2017-12-14

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