SPME-GC-MS分析黄绿蜜环菌挥发油成分.pdfVIP

第54卷第1期精细化工中间体Vol.54No.1

2024年2月FINECHEMICALINTERMEDIATESFeb.2024

分析与测试

SPME-GC-MS分析黄绿蜜环菌挥发油成分

苏婉，王安平，凯迪尔古丽·麦麦提尼亚孜，吐妮萨姑丽·麦麦提艾力，边鹏，庞娟侠，王俊龙*

（伊犁师范大学天然产物与应用重点实验室，新疆伊宁835000）

摘要：利用顶空固相微萃取-气相色谱-串联质谱方法(SPME-GC-MS)分析黄绿蜜环菌的挥发油成分，构

建快速鉴定黄绿蜜环菌挥发油成分分析方法。从黄绿蜜环菌挥发油中鉴定出烷、酯、酮、酸、醛等52个成

7-已基二十烷(10.57%)等。为黄绿蜜环菌的进一步研究及开发利用提供了理论依据。

关键词：SPME-GC-MS；黄绿蜜环菌；挥发油；定性分析

中图分类号：R282文献标志码：A

D0I:10.19342/ki.issn.1009-9212.2024.01.018

AnalysisofVolatileOilCompositionofArmillariaLuteo-virensbySPME-GC-MS

SUWan,WANGAn-ping,KADIRGULMamatnyaz,TUNSAGULMamatali,BIANPeng,PANGJuan-xia,WANG

Jun-long*

(KeyLaboratoryofNaturalProductsandApplications,YiliNormalUniversity,Yining835000,China)

Abstract:ToconstructananalyticalmethodforrapididentificationofvolatileoilcomponentsofArmilarialuteo-

virens.TheSPME-GC-MSmethodwasemployedtoanalyzethevolatileoilcomponentsofSPME-GC-MS.Atotalof

52compoundswereidentified,accountingfor65%ofthetotalnumberofchromatographicpeaksand98.63%ofthe

totalpeakarea.Thesecomponentsmainlyconsistofalkanes,esters,ketones,acids,aldehydes,andothers.Thereare

11maincomponents,includingbutyldiethylborane(4.26%),2-methyldodecane(4.87%),methylcyclopentane

undecanoate(3.24%),palmiticacid(7.87%),n-hexadecane(6.74%),hexylcyclopentane(5.43%),n-heptadecane

(6.24%),2,9-dimethyldecane(8.42%),methyllinoleate(10.94%),2-methyleicosane(12.23%),and7-hexyleicosane

(10.57%).ThesefindingscontributedtoabetterunderstandingofthevolatilecomponentsofArmillarialuteo-virens

andprovideatheoreticalbasisfortheresearchanddevelopmentofrelatedfoods,healthproducts,anddrugs.

Keywords:SPME-GC-MS;Armillarialuteo-virens;volatileoil;qualitativeanalysis

中国是世界上最早利用食用菌的国家，如《齐方及保健应用均有详细记载[2-3]。黄绿蜜环菌