热压温度对PZN-PZT,PVDF压电复合材料微观结构和性能的影响.pdfVIP

PHBV/PCL 共混体系的相容性研究/王细建等 ·25 · 热压温度对PZN-PZT/PVDF 压电复合材料微观结构和性能的影响* 1,2 1 1 1,2 1 晏海霞 ，胡 珊 ，戴 雷 ，姜 磊 ，宗庆坤 (1 中国地质大学材料科学与化学工程学院，武汉430074 ；2 中国地质大学研究生院，武汉430074) 摘 要 采用固相法合成了PZN-PZT 压电陶瓷材料，再采用溶液混合法制备不同热压温度的PZN-PZT/PVDF （铌锌 锆钛酸铅/聚偏二氟乙烯）压电复合材料，所得材料具有良好的介电和压电性能。采用SEM 观察了PZN-PZT/PVDF 压电复 合材料微观结构，并研究和分析了热压温度对压电复合材料电学性能的影响。结果表明，随着热压温度的升高，复合材料内 部致密度提高，气孔率降低；当热压温度为180～190℃时，压电复合材料缺陷最少，排列最密实，其介电和压电性也最好。 关键词 热压温度 微观结构 介电性能 压电性能 Effect of Hot-pressing Temperature on the Microstructure and Properties of PZN-PZT/PVDF Piezoelectric Composites 1,2 1,2 1 1,2 1 YAN Haixia ，HU San ，DAI Lei ，JIANG Lei ，ZONG Qingkun （１Faculty of Materials Science and Chemical Engineering, China University of Geosciences, Wuhan 430074 ； 2. Graduate School, China University of Geosciences, Wuhan 430074) Abstract PZN-PZT piezoelectric ceramics are fabricated through the solid phase synthesis. PZN-PZT/PVDF piezoelectric composites with different hot-pressing temperatures are prepared by solution-mixing method, and a higher dielectric and piezoelectric properties of the piezoelectric composite are obtained. The microstructure of PZN-PZT/PVDF piezoelectric composites is investigated with SEM, and the effect of hot-pressing temperature on electric properties of the composite is studied. The results show that with the increase of hot-pressing temperature, the interior density of composites increases and the pore ratio decreases, and piezoelectric composites hot-pressed at 180～190℃ have the compactest structure and best dielectric and piezoelectric properties. Key words hot-pressing temperature ，microstructure ，