影响微波辐照脱硫过程因素的试验研究.pdf

( ) 第 32 卷 第 6 期 　 　　　华 　中　科 　技 　大 　学 　学 　报 自然科学版 　　　　　Vol. 32 　No. 6 2004 年 　6 月 　　 　J . Huazhong Univ. of Sci. Tech. (Nature Science Edition) 　 　 　J un. 　2004 影响微波辐照脱硫过程因素的试验研究 隋建才 　丘纪华 　程 　荣 　程纪东 (华中科技大学 煤燃烧国家重点实验室 , 湖北 武汉 430074) 摘要 : 应用微波辐照方法 ,采用单因子法考察了微波照射时间、煤粉粒径 、浸提剂等因素对黄铁矿向磁黄铁矿 转化效果的影响. 并应用正交试验考察各因素对黄铁矿转化效果的综合影响 ,优选出黄铁矿转化的最佳工艺 条件为 :微波辐照 3 min 、加 NaOH 浸提剂 、煤粉粒径为 0. 086～0. 102 mm ,此时转化率可达到 45. 7 %. 关 　键 　词 : 煤粉 ; 脱硫 ; 微波辐照 ; 因素分析 中图分类号 : T K16 　　文献标识码 : A 　　文章编号 : (2004) Experimental study of the influence of desulf urization by microwave radiation S ui Jiancai 　Qiu Jihua 　Cheng Rong 　Cheng Jidon g Abstract : The high sulfur coal was treated under microwave radiation. The effect of treating condition , in cluding irradiation time , the size of pulverized coal , and additive substance (Na CO , NaOH and CuCl · 2 3 2 2H O) on the conversion rate of p yrite was studied by single factor method. The Orthogonal design method 2 was used to explore these factors of influencing the conversion rate of p yrite , and the optimal treating condi tions of conversion by microwave radiation obtained. The optimum conditions are that treatment time is 3 min , the range of the particle size is from 0. 008 6 to 0. 102 mm , and sodium hydroxide is used as additive so that the conversion rate of p yrite can reach up to 45. 7 %. Key words : pulverized coal ; desulfurization ; irradiation by microwave ; factor analysis Sui Jiancai 　Doctoral Candidate ; State Key Lab. of Coal Combust