快速测定植物提取物中的汞.pdfVIP

4 5 Vol. 4 No. 5 2013 10 Journal of Food Safety and Quality Oct. , 2013 * 张 遴 , 王文瑞 (, 710068) 摘 要: 目的 方法 , , 结果 GB/T 5009.17-2003 , 0∼1000 ng, 0.430 µg/kg(RSD)3.5%, 93.5%∼102.8%结论 , , 关键词: ; ; Rapid determination of mercury in plant extract * ZHANG Lin , WANG Wen-Rui (Shaanxi Entry-Exit Inspection and Quarantine Bureau, Xi ’an 710068, China) ABSTRACT: Objective To establish a rapid determination method of mercury in the plant extract. Methods a direct mercury measurement technology, which could directly determine the samples without any pretreatments was used, and the instrument conditions were optimized. Finally detection limit, precision and accuracy of this method were researched, etc. Results Compared with the national standard GB/T 5009.17-2003 and validation of the national standard substance, the linear range of this method was 0~1000 ng, and the lowest detection limit was 0.430 µg/kg. Its relative standard deviation (RSD) was within 3.5% and the recovery was 93.5%~102.8%. Conclusion To determine the mercury in our national reference material such as tea, cabbage patch, and spi- nach, the values were all within the standard range of values. This method is suitable for the rapid determina- tion of plant extracts of mercury. KEY WORDS: mercury; direct mercury analyzer; plant extract , 1 引 言