热脱附-气相色谱_质谱法检测食品接触材料中有机残留物.pdfVIP

4 4 Vol. 4 No. 4 2013 8 Journal of Food Safety and Quality Aug. , 2013 -/ 熊中强, 杜 宇, 庞 震, 李宁涛* (, 300042) 摘 要: 目的 / 方法 /, , 结果 92.7%~112.5%, 3.3%, R20.9890, 0.07~0.11 mg/L结论 , 关键词: ; ; /; Determination of organic residuals in food contact materials by thermal desorption-gas chromatography/mass spectrometry * XIONG Zhong-Qiang, DU Yu, PANG Zhen, LI Ning-Tao (Technical Center for Safety of Industrial Products, Tianjin Entry-Exit Inspection and Quarantine Bureau, Tianjin 300042, China) ABSTRACT: Objective To develop a gas chromatography/mass spectrometry method for determination of organic residuals in food contact materials. Methods The organic residuals in food contact materials were determined by thermal desorption gas chromatography using mass spectrometry detector. Theorganic residuals were characterized according to retention time and was quantitatively determined by external standard method. Results Recoveries of typical organic residuals were between 92.7%~112.5% with RSD less than 3.3%, R20.9890, and limit of detection ranged from 0.07~0.11 mg/L. Conclusion This method is sensitive, accu- rate and precise and it is suitable for the detection oforganic residuals in many kinds of materials. KEY WORDS: food contact materials; organic residuals; gas chromatography/ma