微波预处理-超临界CO2萃取高品质茶籽油的工艺研究.pdfVIP

王 艺 }支求 食品摹亚斜技 ，．35，No．24，2014 微波预处理一超临界Co2萃取 高品质茶籽油的工艺研究 黄闪闪 ，吴苏喜1I2-，谭传波’ (1．长沙理工大学化学与生物工程学院，湖南长沙410114； 2．湖南博邦农林科技股份有限公司，湖南常德 415700) 摘 要：为保证超临界萃取技术高效萃取高品质茶籽油，运用微波前处理加以辅助，利用正交设计得到最佳微波处理 条件为：原料水分7．8％，粉碎粒度为过100目筛，微波处：~Y-120s。再用响应面法对其苹取压力、温度和时间等工艺条件 进行了优化分析，得到最佳工艺条件为：在33MPa压力和45℃温度下连续萃取时间2h。此条件下的萃取效率高达 92．76％，远高于未经微波处理的方法。该工艺所得茶籽油V。含量高达182．4mg／kg，只需简单脱酸即达到压榨一级茶籽 油标准。 关键词 ：茶籽油，超临界CO萃取，微波，响应面 Studyonthesupercriticalcarbondioxideextractionprocesscombined withmicrowavepretreatmentforefficientlyextractinghighquality camelliaseedoiI HUANG Shan—shan ．W U Su-xi’’．TAN Chuan—bO (1．SchoolofChemistry andBio-engineering，ChangshaUniversityofScience＆ Technology，Changsha410114，China； 2．HunanBobangAgricultureandForestryScienceandTechnologyCo．，Ltd．，Changde415700，China) Abstract：Thesupercriticalcarbondioxideextractionprocesscombinedwithmicrowavepretreatmentforefficiently extractinghigh quality camellia seedoilwasinvestigated．Orthogonaltestwasusedto determinetheoptimal conditionsofmicrowave pretreatment．The optimum process parametersobtained were asfollows：camellia seedflourwithmoisturecontent7．8％ and througha 10Omeshsievewastreatedbymicrowavefor120s．Then the supercriticalcarbon dioxide extraction processwas optimized by response surface methodology．The optimum process parameters obtained were extracting for2h at33MPa and 45oC ．Underthis optimum condition．the oiIextractionefficiencywas9276％ and wasfarhigherthanthatwithoutmicrowaveprocessing method The extracted oilwith a satisfying VEcontentof182．4mg／kg could meettherequirementofthe pressing firstclasscamelIiaoiIfollowe