重氮化反应 氨基变羟基 m-METHOXYBENZALDEHYDE.pdfVIP

Organic Syntheses, Coll. Vol. 3, p.564 (1955); Vol. 29, p.63 (1949). m-METHOXYBENZALDEHYDE [Benzaldehyde, m-methoxy-] Submitted by Roland N. Icke, C. Ernst Redemann, Burnett B. Wisegarver, and Gordon A. Alles. Checked by H. R. Snyder and Frank X. Werber. 1. Procedure A. m-Hydroxybenzaldehyde. In a 2-l. three-necked flask, equipped with a mechanical stirrer, a thermometer, and a 250-ml. dropping funnel, 575 ml. of 6 N sulfu