超细晶粒WC-129％Co热喷涂粉末地制备研究.pdfVIP

第十七届全国热喷涂技术经验交流会论文(CTSC’200S$ 超细晶粒WC-12％Co热喷涂粉末的制备研究 刘金炎，张敬圜，蒋显亮 (中南大学袭面与涂层技术研究所，长沙，410083) 【蘩簧】裁用烧缝磁磷法，戳褪颥救(约3。56淘n)翻越缁鬏较(约0．鑫8撕辩耪、Go粉先主要骧籽铡 备了WC-12％Co热喷涂粉末。用×一射线衍射和扫描电子赶微镜(SEM)对粉末的形貌和结构进行了研究，讨 论了烧结温度、颗救火小、有机粘缩剂、碳粉对粉末特性的影响。实验结果表明：原始粉宋颗粒大小影响 粉泰的烧结状态和榻缀成；添加有机察占缩荆能促进粉末的烧结；添加碳粉主要以游离态存在，可有效抑斑 越纲粒耪烧缝时rl(e耐瞄)等毒害桶的壅凌；{250℃蹙制冬超缯鬟铲{2％Co热嚷涂耪寒较好戆娆结瀑度。 【关键词l热喷涂；趟细晶粒；WC-Co粉；烧结 GrainWC·-12％CoFeedstock ofUltra--fine Preparation PowderforThermal method SprayingbySinter—crushing Lit=Jin-yan，ZhangJing-guo，JiangXian-liang of South (InstituteSurfaceCoatingsTechnology,CentralUniversity,Changsha 410083，China) [Abstract]WC-12％Cofeedstockforthermal Was method． powdef sprayingpreparedbysinter-crushing coarseand ultra-fine carbide andcobalt wereusedaSmainraw 3．569in 0。68ttm tungsten powders powder materials．Theinfluencesofthe binderandcarbon onthe and sintcringtemperature，organic powdermorphology diffractionand electron phasecompositiona他investigatedbyX-ray scanning microscopy．Theexperimental resultsshowthatthe sizeof WC influences and phase panicle Startingpowdersignificantlysintcringprocess addedtheraw theadded binder into carbon，exists constituent，organic powderspromotessintcringprocess,and freestateinthe iseffectivein theformationof other main移in preparedpowd黼and preventing rl(C03WsC)and nODWC isfoundedthat1250℃isthebetter for ultra-fine pha