化学溶液沉积法制备单分散氧化锌纳米棒阵列.pdfVIP

2005 63 Vol. 63, 2005 18 , ACTA CHIMICA SINICA No. 18, · · a *,a a a a a b b a ( 310027) (b 310027) ZnO , ZnO . ZnO , . FESEM, TEM, HRTEM, SAED XRD . ZnO PL , , ZnO , O . ZnO; ; Synthesis of Monodispersed ZnO Nanorod Array Films by Chemical Solution Deposition LUO, Zhi-Qianga ZHANG, Xiao-Bin*,a CHENG, Ji-Penga TAO, Xin-Yonga a a b b LI, Yu LIU, Fu TANG, Xiao-Ming WANG, You-Wen a ( State Key Laboratory of Silicon Materials, Department of Materials Science and Engineering, Zhejiang University, Hangzhou 310027) (b Analysis and Measurement Center of Zhejiang University, Zhejiang University, Hangzhou 310027) Abstract Monodispersed and well-aligned ZnO nanorod arrays have been synthesized by chemical solu- tion deposition on spin-coated and preheated ZnO sol films. The diameter of ZnO nanorods was controllable by adjusting the process of nano-ZnO film substrates. The morphology and crystalline structures of ZnO nanorods were characterized by field emission scanning electron microscopy (FESEM), transmission elec- tron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED) and X-ray diffraction (XRD). The room temperature photoluminescence spectrum of the