傅立叶变换红外光谱法分析食品及油脂中反式脂肪酸.pdfVIP

248 2008 2 18 2 C inese Journal ofH ealt Laboratory Tec nology, Feb 2008; V ol 18 No 2 傅立叶变换红外光谱法分析食品及油脂中反式脂肪酸 1 1 1 1 1 2 倪昕路 , 韩丽, 王传现, 周瑶, 郭德华 , 董建华 ( 1, 200135; 2(), 201206) [ ] : : ( HATR) ZnSe, ( DTGS) 966 cm- 1 , : : , [ ] 食品及油脂; 反式脂肪酸; 水平衰减全反射(HATR); 氘 三甘氨酸硫酸酯( DTGS) 检测器 [ ] O65733 [] A [] 1004- 8685( 2008) 02- 0248- 03 Determ ination of trans fatty acid in food and oil by fourier transformation infrared spec trom eter 1 1 1 1 1 2 N i X inlu , H an L i , Wang Chuanx ian , Zhou Yao , Guo D eh ua , D ong J ianhua ( 1S ang ai Export and Im port Inspection and Quarantine, S ang ai 200135, C ina; 2T erm o Fis er Scientific L td, Co, S ang ai 201206, C ina) [ Abstract] Objective: To determ inae contents of trans fatty acids in food and oil by FT- IRM ethods: Fat extracted from food and oil samp le was determ ined directly on t e ZnSe crystal cisterna of orizon attenuation total reflection ( HATR) equ ipm entw it deu terated triglycine sulfate detector ( DTGS) in t e FT- IRQualification w as accom plis ed t roug c aracteristic absorption of trans- doub le band at 966 cm- 1C alcu late t e percent content of trans fatty acids isom ers in oil by t e standard curve of t e peak area to t e content of trans fatty acidR esults: T is m et od quantitated trans fatty acids in food and oil acuuratly by t e c aracter istic absorption of trans- double bandConclusion: T em et od is smi ple, qu ick, accurate and can be applied to t e nutrition la belm ak ing [ Key w ords] Foods and O i;l Trans fatty acids; H orizon attenuation total reflection (HATR); Deuterated triglycine su lfate de tector ( DTGS) detector , , , , , , ( trans- fatty acids, TFA