微波消解_电感耦合等离子体原子发射光谱仪测定面制食品中的铝_杨雪娇.pdfVIP

S cience and T echno logy of Food Ind ustry , , , , (东莞出入境检验检疫局, 广东东莞 523072) ) , : 采用全自动微波消解仪对样品进行前处理, 消解液用 ICP 进行检测讨 了微波消解程序对样品的影响, 及 ICP 光 , 谱条件对测试结果的影响表明在最高温度为 180 时消 5~ 9[ 6] 解 30m in, 最佳光谱条件为: 308215nm, RF 功率为 1150kW, 载气压力为 017MPa 时, 曲线线性相关系数为0999, 检出 限为 021g /mL, 回收率为 917% 测定结果令人满意 : 铝, 面制食品, 微波消解, ICP [ 7, 8] , A bs trac:t F irs he s am p le w as d ecom p os ed w ih he fu ll , , a u om a ic m ic row ave , a nd he n ana yl z ed b y he IC PThe in fluenc e o f he p rog ram o f m ic row ave a nd , , he cond i ion o f s p ec rum w e re d is cu ss edI s how ed w he n he s am p le w as d ecom p os ed fo r 3 0m ni in he , h gi he s em p e ra u re 180 , he b e s co nd i oi n o f , , s p ec rum w as 308215 nm, he p ow e r o f RF w a s 115 0kW, he s res s o f ca rrie r ga s w as 0 17MPa, he 1 linea rly d ep end e n c oe ff ic ien o f he c u rve w a s 09 999, he de ec oi n lmi i w a s 021g /m L, he 11 reco ve ry w a s 917% The e s re su l is sa isf ied , Key w o rds: A lum in ium; food s u f f m ad e b y f lo u r; m ic row ave; IC P 1000g /mL, 10% ( V /V ) ; ; : T S2132 : A : 1002- 0306( 2007) 09- 0206- 03 ( 182s / cm ) ETHOS PLU S M iles one; ICP- AES , 773% [ 1] ( PROF ILE ) Leem an , 12