溶剂浸取法提纯磷脂酰胆碱的工艺研究.pdfVIP

28 4 Vol28No4 2009 12 Journal of Wuhan Polytechn ic Un iversity Dec2009 : 2009) 0400090 DO I: 10. 39 9/j. issn. 2009. 04. 003 溶剂浸取法提纯磷脂酰胆碱的工艺研究 ( , 351254) : 为了提高磷脂产品中磷脂酰胆碱的含量, 试验用乙醇为溶剂浸取提纯浓缩大豆磷脂, 以产品的磷脂酰胆碱含量与 率为标准, 用单因素法和正交设计法分别研究乙醇浸取过程, 优 化了工艺参数, 即: 浸取温度 35 , 乙醇浓度 90%, 浸取时间 15 m in, 溶剂用量为 8mL /g大豆 磷脂, PC 的含量可以从原料中的 22. 70% 提高到 54. 75%, PC 率超过 99. % 乙醇浸取物 在 5 温度下, 用 7mL /g乙醇浸取物用量的丙酮浸取 3次, 可得到PC含量为 70. 80% 的粗 磷脂, PC 率高达 97. 2%, 杂质去除率达 93. % : 浓缩大豆磷脂; 溶剂浸取; 磷脂酰胆碱; 含量 : TS 221 : A Resea rch on the techno logy of purify ing phosphatidy lcho line in the so lvent- extract ion met hod CA I Junx iu ( Chem icalEngeneering Department of Fujian M eizhou Bay Technical College, Putian, 351254 , Ch ina) Ab stract: In order to mi prove the phospholip id content in the product phosphatidylcholine, Ethanol is tested as solvent extraction purification of concentrated soybean lecithin. It takes the phosphatidyl choline content and reclami ing rate as a standard, and uses single- factormethod and orthogonal design m ethod to study respectively the ethanol mi mersion process to optmi ize the process param eters, namely: extraction temperature 35 , ethanol concentration 90%, leach ing tmi e, 15 m in, solvent dosage 8mL / g soybean, lecithin, PCs content can be from 22. 70% of raw m aterials to 54. 75% , PC reclami ing rate as h igh as 99. %. Ethanol leaching extract the temperature at 5 , using - 7mL / g ethanol leaching extract volume of acetone leaching three tmi es, availab ility of PC content of 70. 80% of the crude p