左氧氟沙星印迹聚合物微球及其特异吸附特征.pdfVIP

0 [1] [2-3] [4-5] [6-7][8-9] 1 1.1 Perkin-Elmer 983 Norwalk JSM-5610LV JEOL KQ2200B DZF-6051 SHA-B TGL-20B T6 Levofloxacin LVFX MAA Acros EDMA Acros AIBN AIBN 1.2 MIP NIP MIP NIP 4000-400 cm-1 1.3 0.3 mmol LVFX 50 ml MAA 1.8 mmol 4 12 h6mmol EDMA 30 mg AIBN 8 min 60 24 h 10% / 1.4 1.4.1 l0 ml 20 mg MIP 5 ml 4.0 mmol/LLVFX 25 10000 r/min10 min 300 nm LVFX (1) Q = (C1-C2) ×V×1000/MMIP (1)Q (μmol/g) C1 C2 (μmol/mL) V (mL) MMIP (mg) 1.4.2 l0 ml 20 mg MIP 5 ml LVFX 25 2 h 10000 r/min LVFX (1)MIP Q 1.4.3 1