常压水解法制备纳米二氧化钛及表征.pdfVIP

无机盐工业 第 42 卷第 6期 42 INORGAN IC CHEM ICALS INDUSTRY 20 10年 6月 1 1 2 2 1 , , , , ( 1. , 3004 10; 2. ) : , , , , : 12, 40 g/L, 50 g/L; , 85 5 , 2 h, pH 2; , , 1; 85 2~ 3 h, 700 2 h, , 7~ 13 nm : ; ; ; : TQ134. 11 : A : 1006- 4990( 2010) 06- 0042- 02 Preparation and characterization of nano- sized T iO2 by atm ospher ic hyd rolysis m ethod 1 1 2 2 1 Zha Yanyu , L iY ng , Shang L iandi , W angHu ihu i, Yuan Y ingx ian ( 1. T ianj in Vocational Institute, T ianj in 300410, Ch ina; 2. CN OOC T ianj in Chem ical R esearch D esig n Institute) A b stract: Optmi um c nditi ns f preparing nan - sized titan ium di x ide ( T iO ) p wder by atm spheric hydr lys is 2 m eth d were stud ied, in w hich the interm ed iate pr duct titanyl su lfate ( T iOSO ) fr m industrial titanium d i x ide pr ducti n 4 w ith su lfu ric acid pr cess and industrial ureaw ere used as raw m aterials. M aj r influencing fact rs, such asm ass c ncentra ti ns f titanyl sulfate and urea, as w ell as am un-t -f substance rati f titanyl su lfate t urea in pr ducti n pr cess f nan- sized T iO w ere investigated. Acc rding t expermi ental param eters, ptmi um pr gram f r preparati n f nan- sized T iO w as 2 2 btained. N am ely, am un t- f- substance rati f T iOSO t CO ( NH ) w