毕业设计（论文）-丝网印刷工艺对掺杂氧化铈基极限电流型氧传感器的性能影响.docVIP

毕业论文 题 目：丝网印刷工艺对掺杂氧化铈基极限电流型氧传感 器的性能影响 学生姓名： 学 号：1161142129 专 业：无机非金属材料工程 班 级：无机一班 指导教师： 丝网印刷工艺对掺杂氧化铈基极限电流型氧传感器的性能影响 摘 要 随着我国经济实力的快速增长，伴随产生的环境、资源、社会伦理道德等问题也日益突出。为了达成可持续发展的愿景。我们课题组所研究的氧传感器恰好响应了国家的号召。当然也具有较好的前景。本篇论文使用LaNi0.6Fe0.4O3（LNF）La1-xSrxCo1-yFeyO3（LSCF） 制备固体电解质材料Ce0.8Sm0.2O1.9（SDC） 采用溶胶凝胶法制备了致密扩散障碍层粉体LNF和LSCF，应用X射线衍射分析仪（XRD）对粉体物相进行了表征。并且在查阅相关文献的条件下，制备出LaNi0.6Fe0.4O3（LNF）La1-xSrxCo1-yFeyO3（LSCF） 将烧结好的SDC陶瓷片，用砂纸打磨粗糙后，再用松油醇研磨的LNF或LSCF浆料涂刷在SDC陶瓷片上，再进行烧结即可。尔后利用扫描电子显微（SEM）、电化学工作站对其进行断面结构分析和电化学性能分析 关键词：氧传感器；极限电流；SDC；致密扩散障碍层；LNF;LSCF Silk screen printing process for doped cerium oxide base of limiting current type oxygen sensor device performance impact Abstract With the rapid growth of China’s economy , the constant improvement of the comprehensive national power and our country in the world’s superpower status. At present, the research studied the oxygen sensor just responded to the call of the state. the dense oxygen diffusion barrier layer of limiting current type oxygen sensor has higher sensitivity and wider measurement range, the response speed is faster and better stability than before. In the paper, the solid electron-ion mix conductor material LaNi0.6Fe0.4O3（LNF）and La1-xSrxCo1-yFeyO3（LSCF）is used as materials of dense diffusion barrier of sensors and the dense diffusion barrier limiting current oxygen sensor was developed successfully through the technology of Pt liquid agglutination, and oxygen sensitivity is tested by limiting current oxygen sensor testing equipment. The solid electrolyte material Ce0.8Sm0.2O1.9(SDC) is prepared by sol-gel method. X-ray powder diffraction(XRD), scanning electron microscope(SEM) were applied to characterize the compositions and morphologies of the powder. The sintering shrinkage and sintered density are studied. The SDC solid electrolyte ceramic material has been prepared . The dense diffusion barrier material LSCF and LNF is prepared by sol-gel method. The compositions and morphologies of the powder are char