鱼体中两种挥发性有机残留物的提取和检测.pdfVIP

2012中国食品与农产品质量安全检测技术应用国际论坛 2012ChinaFoodand Products Exhibition AgriculturalQualitySafetyTestingTechnology 鱼体中两种挥发性有机残留物的提取与检测 战培荣王海涛陈中祥刘伟 (中国水产科学研究院黑龙江水产研究所；农业部渔业环境及水产品质量监督检验测试中心 (哈尔这)哈尔滨1 摘要鱼体中挥发性残留有机物的提取和分析是检测领域重点关注和研究的问题。由于鱼体本身 组成较特殊，胶体蛋白和不饱和脂肪酸等含量较高，传统的提取水中挥发性有机物的蒸馏方式不能 满足提取鱼体中挥发性有机残留物的需要。挥发酚和硝基苯是重要的有毒、有害污染物。本文实验 研究了水蒸汽蒸馏方法提取鱼体中挥发酚和硝基苯的效果，研究了鱼体中挥发酚和硝基苯残留量的 测定方法。结果表昵水蒸汽蒸馏提取法效果好，方法实用，便于操作，适用于处理后样品的分析测定， 已应用于鱼体中挥发酚和硝基苯残留量的测定。 关键词鱼，挥发酚，硝基苯，水蒸汽蒸馏法，提取，残留检测 The and twovolatile residueinfish extractiondetectionof organic Zhan Wei Peirong，WangHaitao，ChengZhongxiang，Liu riverfisheriesresearchinstitute，Chineseoffisheries (Heilongjiang academy environmentand centerofthe of Harbin， supervisiontesting ministryAgriculture aquaticproductquality 150070 china．E·mail：zhanpr@yahoo．com．cn) AbstractTheextractionand ofvolatile residuesinfish is on analysis organic bodykeyquestion areasofresearchand fish itself is andthe body compositionspecial，colloidalproteins inspection．Since unsaturated is watervolatile distillation acidcontent fatty higher,traditionalextracting organiccompounds cannotmeetfish volatile residuesneeds．Thevolatile andnitrobenzeneare extract organic phenols environment methodofvolatile andnitrobenzeneresidueinfish important pollutant．Theanalyse phenols is becausethehealthof wereharmedtoeat thefish。The bodyveryimportant people polluted