对_中国药典_川木通药材薄层鉴别方法改进.pdfVIP

m ethod s wa s p erform ed on a D iamon sil C18 co lum n gradien t elu ted w ith aceton itrile005 mol/L KH2 PO4 (pH3 w ith H3 PO4 ) at the flow rate of 08 m l/m in The temp eratu re of co lum n wa s 25 ℃ and the UV detection wavelength wa s 270nm R esu lts: The HPLC fingerp rin t of Rh izom a Cop tis, show ing 16 characteristic p eak s, wa s estab lished from 10 lots of Rh izom a Cop tis By comp arision of the reten tion tim e and the online UV sp ectra of chem ical standard s, p eak 11, 12 , 13, 14 and 15 were iden tified as Ep iberberine, J atrorrh izine, Cop tis