无机材料科学基础Ⅱ.ppt

无机材料科学基础Ⅱ 实验指导书 于金库 无机材料的综合热分析（DSC/TG） 一、实验目的与任务 二、仪器结构原理及特点 工作原理图： TG-DSC/DTA及Cp支架示意图 主要技术参数： 温度测量范围 -120～1650 ℃(不同炉型) 比热测量温度范围 室温～1400 ℃ 比热测量精确度 ≈5% 比热测量范围 0.1～5.0 J/gK 基线重复性 ≈1 ?V(±2.5mW) 噪声影响(最大) ≈15 ?W(和温度有关) 基线线性漂移 3 ?V 温度精度 1 K 热焓精度 ±3% 真空度 10-2 Pa 吹扫气氛 氧化性气体，还原性气体，惰性气体 ,带走产生的毒性、可燃气体 热重精度 10－6 g 三、实验方法 （二）样品准备 （三）开机 Sample 测试模式 Sample+Correction 测试模式 四、实验数据处理 DSC/DTA 部分分析功能： 五、思考题 六、操作注意事项： 实例分析：Al2O3，石英砂与 CaCO3 混合物成分分析 The X’Celerator is the world’s fastest X-ray detector. The data collection can be carried out much faster, because of the use of RTMS (Real Time Multiple Strip) detection technology. It is like having over 100 parallel detectors in the diffractometer, instead of just one. As a result of this, an increase in speed of datacollection with a factor of up to 100 is routinely achieved. Unlike competitor’s ‘fast’ detection systems, this increase in speed of data collection is not accompanied with a decrease in resolution. Even better, when a high speed of data collection is not required, a scan with a superior data quality can be obtained in the same time. The detection system is mounted on a PreFIX module and can easily be exchanged for other PreFIX modules when other types of experiments are to be performed. There is no need for laborious re-alignment procedures. The use of RTMS detection technology allows for a simple module that does not require any additional calibration or maintenance. The X’Celerator is the world’s fastest X-ray detector. The data collection can be carried out much faster, because of the use of RTMS (Real Time Multiple Strip) detection technology. It is like having over 100 parall